A Report
Scientific Highlights.
This was the thirtyfifth teaching event in the field of Crystallography organized
by the contractor at the Ettore Majorana Centre, Erice, Italy, during the last
thirty years.
The scientific programme was organized as a logical progression: fundamentals,
strategies and techniques for the preparation of crystal forms ("polymorphs"),
procedures for their identification and characterization, importance of polymorphs
in different industrial chemical environments (high-energy materials, pigments
and dyes, pharmaceuticals), a number of real-life scenarios and case studies
from these industries, and finally the importance and ramifications of intellectual
property considerations in the development and use of different crystal forms.
The qualified professional origins of the lecturers for these topics (they were
invited two years in advance, one only justifying the withdrawal with his age!)
and the manner in which they covered the material is exemplary of the interdisciplinary
nature of Polymorphism and its growing importance in both industrial and academic
research.
F. Herbstein (Technion, Israel), a veteran crystallographic practitioner, opened
with an historical survey, raising many of the questions subsequently addressed
in the remainder of the event. L. Yu (Univ. of Wisconsin) laid out the thermodynamical
principles and J.O. Henck (Bayer, Leverkusen) demonstrated how thermodynamical
variables are conveniently summarized in an energy-temperature diagram. R. Boese
(Univ. Essen) showed how thermomicroscopic methods could facilitate the identification
and characterization of polymorphs. S. Reutzel (Eli Lilly Co., Indianapolis)
described methods to obtain precise measurements of thermodynamic properties.
Once the groundwork had been prepared with the fundamental issues, practical
examples and workshops, a number of lecturers (A. Gavezzotti, Univ. Milan; S.
Price, Univ College, London; M. Ward, Univ. Minnesota, Minneapolis) described
their advanced research results and headed hands-on afternoon workshops. The
last two afternoons were devoted to very dynamical, open "Ask the Experts"
sessions, chaired with charm and competence by S. Byrn (Purdue Univ., West Lafayette).
Participants were invited to pose any kind of relevant questions (anonymously,
if desired) to all of the event lecturers who were also present in the hall.
The first of these sessions turned into a rather lively higher level discussion
among the lecturers, which led to some criticism from the students. The second
session therefore was devoted exclusively to questions raised by students, who
benefited greatly by this exposure to recognized experts and personal attention
to their questions and practical problems.
In order to give students a chance to present their own work they were encouraged
to submit abstracts, most of which were exhibited at two evening poster sessions.
In addition, twelve abstracts particularly relevant to the general lecture for
a specific day were chosen for oral presentation of 20-30 minutes (Gervais,
Dziubek, Van de Streek, Pulham, Schmidt, Gilardi, Wu, Dova, Comotti, De Matos,
Grassman, Broder).
There was a diffused interaction with participants in the parallel meeting on
Electron Crystallography, and some participants liked to shift sometimes from
one meeting to the other dependent on the interest. The two crowds with basic
different interests had nevertheless several occasions - see common lectures
and social events - to exchange views producing an efficient way of uncommon
scientific interaction.
The overall atmosphere in the course was particularly informal and friendly,
which led to the establishment of many new personal and professional contacts
and the opportunity for scientific collaboration. The shared Erice experience
is one with long lasting effects, as course participants always recognize a
bond formed during the course, and this bond can foster scientific contacts
many years beyond the formal dates of the course. Ever so often, young students
at the Erice crystallographic meetings become leaders, lecturers and even directors
of future events.
The hands-on sessions (for which 23 PCs had been rented, a major expenditure
under Cost Category D) received some criticism, mainly related to local conditioning
of space and time: however, the facilities for running multiple sessions overlooked
with dedication and perseverance by John Irwin, UCSF, USA, have called for much
praise.
European Added Value (incl. Networking).
Nationals from EC and Associated States were an overwhelming majority. Six European
nationals working outside EC Countries have been attracted. Several contacts
have produced further collaboration, e.g. the uncommon talk on polymorphism
of fats included in chocolate has provoked a lot of discussion and exchange
of views with the dutch group, Laboratorium voor Kristallographie, Amsterdam,
well represented by a young greek scientist, Eva Dova, a PhD graduated in Amsterdam.
Invitations to present the lecture elsewhere and collaborative projects have
thereafter initiated this new field for Crystallography.
Another exciting achievement, improved after the pioneering initiative in the
Event no. 1 of this series, has been the web broadcasting. The proceedings were
viewed to some extent from at least 10 countries (USA, UK, France, Canada, Belgium,
Poland, Japan, Russia, India, Italy) and by up to 10 labs at one time. The lectures
have been recorded, placed on the web and DVD edition distributed to those requesting
them.
In addition, several opportunities have been offered in order to provide an
effective route to social and multi-disciplinary scientific dialogue between
novices and experts. The 30th anniversary celebration of the crystallographic
activity at the Majorana Centre, a Treasure Hunt "battled" within
the limited borders of the town, was a major event in this respect.
Additional Information.
The success of the Meeting is best expressed in terms of the answers to a three-pages
questionnaire distributed and anonymously filled - this is our habit since 1978
- by participants before leaving. On ten questions related to purposes and successes
(two different groups of scores for them), where the score varied from 0 to
4, the average of the twenty averages, our figure of merit, is 3.44 outbreaking
the previous top scores of 3.39 and 3.27 reached in the years 2003 and 2002,
respectively. This fits with the result observed when they were asked "How
do you score (0 to 100, 100 maximum) the overall value of the meeting to you?"
: the average figure from seventysix (invited speakers and "students")
answers is 89.8; the top reached in the past was 88 !
Awards of a book, authored by J. Bernstein on Polymorphism, were assigned to
the two most attractive poster presentations.